Journal of Inorganic Materials, Volume. 38, Issue 11, 1257(2023)
As a high-temperature-resistant structural reinforcement material with excellent performance, alumina continuous fiber has been widely used in various fields. However, its large-scale preparation is still a great challenge due to the technical difficulty. Herein, the alumina continuous fibers were prepared using self-made aluminum sol and commercially available silica sol as precursors, in which the microstructure and composition of aluminum sol were studied to reveal their excellent spinnability. Preparation of alumina-based gel continuous fibers with length longer than 1500 m was realized by Sol-Gel combined dry spinning technology. After calcination at 1100 ℃ for 30 min, the continuous ceramic fiber composed of γ-Al2O3 and amorphous SiO2 with the diameter and mean tensile strength of 10 μm and 2.0 GPa was successfully obtained. Microstructure analyses revealed high relative density of the ceramic fibers, in which the γ-Al2O3 nanocrystals with size of 10-20 nm uniformly distributed in amorphous SiO2, resulting in excellent mechanical properties. This preparation process is environment-friendly, simple and controllable, showing great potential in practical application. The test for high temperature resistance revealed that the alumina continuous fiber can work for a long time at 1000 ℃ while it can endure as high as 1300 ℃ for a short-time service.
Get Citation
Copy Citation Text
Yuna JIA, Xu CAO, Xiuling JIAO, Dairong CHEN.
Category:
Received: Mar. 27, 2023
Accepted: --
Published Online: Mar. 6, 2024
The Author Email: CHEN Dairong (cdr@sdu.edu.cn)