Journal of Inorganic Materials, Volume. 38, Issue 2, 170(2023)

Effect of Recombination Time on the Structure and Properties of P2O5-Al2O3 Heterogeneous Composite Glass

Qingong ZHU*... Gaoling ZHAO and Gaorong HAN |Show fewer author(s)
Figures & Tables(9)
XRD patterns of samples prepared with different recombination time (a) and recombination time of 10 min (b) with inset showing optical photo of the sample
FT-IR spectra of P2O5-Al2O3 matrix glass (a) and SiO2-Na2O high-silicate glass (b)
AFM-IR images of the matrix glass (a) and heterogeneous composite glass prepared with different recombination time (b-f)
High-resolution P2p XPS spectra for heterogeneous composite glass fitting with the least squares method
High-resolution O1s XPS spectra for heterogeneous composite glass fitting with the least squares method
Raman spectra of P2O5-Al2O3 heterogeneous composite glass prepared with different recombination time
Young's modulus of P2O5-Al2O3 heterogeneous composite glass prepared with different recombination time
  • Table 1. Peak positions, full width at half maximum (FWHM) and area from the fitting curves of P2p core levels for heterogeneous composite glass

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    Table 1. Peak positions, full width at half maximum (FWHM) and area from the fitting curves of P2p core levels for heterogeneous composite glass

    Recombination timePeak position/eVFWHM/eVArea/%
    Main peakDeconvoluted peak
    10 s134.46134.231.4666.7
    135.171.4733.3
    2 min134.42134.221.4166.7
    135.171.4133.3
    4 min134.59134.351.4766.7
    135.281.4433.3
    6 min134.67134.361.7466.7
    135.602.1633.3
    8 min134.44134.261.4566.7
    135.181.5033.3
  • Table 2. Peak positions, full width at half maximum (FWHM) and area from the fitting curves of O1s core levels for heterogeneous composite glass

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    Table 2. Peak positions, full width at half maximum (FWHM) and area from the fitting curves of O1s core levels for heterogeneous composite glass

    Recombina-tion time NBO-Li/MgNBO-AlBO
    BE/eVFWHM/eVArea/%BE/eVFWHM/eVArea/%BE/eVFWHM/eVArea/%
    10 s531.931.3929.69532.361.3929.68533.351.7840.63
    2 min532.101.4337.42532.782.1731.30533.202.1731.29
    4 min531.951.4331.66532.411.9734.18533.291.9734.16
    6 min531.971.3929.65532.361.9935.18533.291.9935.17
    8 min532.071.3531.65532.552.0734.18533.242.0734.17
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Qingong ZHU, Gaoling ZHAO, Gaorong HAN. Effect of Recombination Time on the Structure and Properties of P2O5-Al2O3 Heterogeneous Composite Glass[J]. Journal of Inorganic Materials, 2023, 38(2): 170

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Paper Information

Category: EDITORIAL

Received: May. 20, 2022

Accepted: --

Published Online: Sep. 27, 2023

The Author Email: ZHU Qingong (zhuqingong@zju.edu.cn)

DOI:10.15541/jim20220286

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