Laser & Optoelectronics Progress, Volume. 60, Issue 13, 1330001(2023)

Detection of Tantalum-Niobium Ores Using Double-Pulse Laser-Induced Breakdown Spectroscopy Based on a Single Laser

Shihang Chen1, Li Liu1,2, Zhiwei Deng1, Zhongqi Hao1,2、*, Jiulin Shi1,2, and Xingdao He1,2
Author Affiliations
  • 1Jiangxi Province Key Laboratory of Optoelectronic Information Science and Technology, Nanchang Hangkong University, Nanchang 330063, Jiangxi, China
  • 2Jiangxi Province Optoelectronic Detection Technology Engineering Laboratory, Nanchang Hangkong University, Nanchang 330063, Jiangxi, China
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    Figures & Tables(8)
    Schematic diagram of the experimental setup
    Variation of the intensity of the spectral lines with the amount of defocusing. (a) Reflected light; (b) transmitted light
    Variation of SNR with laser pulse energy: (a) Reflected light; (b) transmitted light
    SNR of elemental characteristic spectral line as a function of the delay time under SP- and DP-LIBS
    Elemental spectral line intensities of LIBS under single and double pulse conditions. (a) Ta; (b) Nb
    Basic calibration curves under SP-LIBS and DP-LIBS. (a) Ta II 263.55 nm; (b) Nb II 269.70 nm
    • Table 1. Contents of Ta and Nb in tantalum-niobium ore samples

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      Table 1. Contents of Ta and Nb in tantalum-niobium ore samples

      Sample No.GBW07154∶GBW07155Ta /(μg·g-1Nb /(μg·g-1
      110∶072.629.6
      29∶1523.2273.4
      38∶2473.1246.4
      47∶3423.0219.2
      56∶4373.0192.2
      65∶5322.9165.1
      74∶6272.8138.0
      83∶7222.8110.9
      92∶8172.783.8
      101∶9122.656.7
      110∶10573.2300.6
    • Table 2. Comparison of quantitative analysis results between SP-LIBS and DP-LIBS

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      Table 2. Comparison of quantitative analysis results between SP-LIBS and DP-LIBS

      ElementR2Detection limits /(μg·g-1
      SP-LIBSDP-LIBSSP-LIBSDP-LIBS
      Ta0.8260.975435.65195.91
      Nb0.9660.990121.9981.79
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    Shihang Chen, Li Liu, Zhiwei Deng, Zhongqi Hao, Jiulin Shi, Xingdao He. Detection of Tantalum-Niobium Ores Using Double-Pulse Laser-Induced Breakdown Spectroscopy Based on a Single Laser[J]. Laser & Optoelectronics Progress, 2023, 60(13): 1330001

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    Paper Information

    Category: Spectroscopy

    Received: Feb. 27, 2023

    Accepted: Apr. 3, 2023

    Published Online: Jun. 29, 2023

    The Author Email: Hao Zhongqi (hzq@nchu.edu.cn)

    DOI:10.3788/LOP230706

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