Laser & Optoelectronics Progress, Volume. 58, Issue 9, 0914002(2021)

Evolution Law of Laser-Textured Microstructure on Ni-Co-Si3N4 Composite Coating Surface

Lingling Ji1, Ninghui Li2, and Min Kang1,3、*
Author Affiliations
  • 1College of Engineering, Nanjing Agricultural University, Nanjing , Jiangsu 210031, China
  • 2College of Transportation Engineering, Nanjing Vocational University of Industry Technology, Nanjing , Jiangsu 210023, China
  • 3Key Laboratory of Intelligence Agricultural Equipment of Jiangsu Province (Nanjing Agricultural University), Nanjing , Jiangsu 210031, China
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    Figures & Tables(16)
    Characterization of the coating surface microstructures. (a) Spherical-cap shaped bump; (b) W-shaped pit; (c) crater pit; (d) pit with double concentric holes
    Surface morphology and cross-section of the coating. (a) 2D morphology image; (b) cross-section
    XRD spectrum of coating
    Top views, 3D images, and contour lines of cross-sections of four typical microstructures
    Characteristic parametric diagrams of the coating surface microstructures at varying pulse energy densities. (a) Diameter; (b) altitude
    Cross-section contour lines of the coating surface microstructures in phase 1
    Cross-section contour lines of the coating surface microstructures in phase 2
    Cross-section contour lines of the coating surface microstructures in phase 3
    Cross-section contour lines of the coating surface microstructures in phase 4
    Characteristic parametric diagrams of coating surface microstructures with varying pulse widths. (a) Diameter; (b) altitude
    Cross-section contour lines of the coating surface microstructures with varying pulse widths. (a) 10-35 μs; (b) 35-50 μs
    Characteristic parametric diagrams of the coating surface microstructures at different numbers of pulses. (a) Diameter; (b) altitude
    Cross-section contour lines of the coating surface microstructures at varying numbers of pulses
    • Table 1. Plating solution composition

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      Table 1. Plating solution composition

      Bath componentMolecular formulaMass concentration / (g·L-1)Specification
      Nickel sulphateNiSO4·6H2O200.000A.R.
      Nickel chlorideNiCl2·6H2O50.000A.R.
      Cobalt sulfateCoSO4·7H2O10.000A.R.
      Boric acidH3BO330.000A.R.
      Sodium dodecyl sulfateC12H25SO4Na0.050A.R.
      ThioureaCH4N2S0.002A.R.
      Silicon nitrideSi3N46.00020 nm
    • Table 2. Laser processing parameters used for experiments

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      Table 2. Laser processing parameters used for experiments

      Number of pulsesLaser pulse width /µsLaser energy density / (J·cm-2)
      110198.73-287.75
      110-50248.47
      1-910211.23
    • Table 3. EDS analysis results of coating

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      Table 3. EDS analysis results of coating

      ElementNiCoSiNCOS
      Mass fraction /%Balance14.230.310.353.630.720.41
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    Lingling Ji, Ninghui Li, Min Kang. Evolution Law of Laser-Textured Microstructure on Ni-Co-Si3N4 Composite Coating Surface[J]. Laser & Optoelectronics Progress, 2021, 58(9): 0914002

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    Paper Information

    Category: Lasers and Laser Optics

    Received: Aug. 24, 2020

    Accepted: Sep. 22, 2020

    Published Online: May. 12, 2021

    The Author Email: Kang Min (kangmin@njau.edu.cn)

    DOI:10.3788/LOP202158.0914002

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