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Journal of Inorganic Materials, Volume. 34, Issue 8, 899(2019)

Synthesis of Zn, Mn doped Fe3O4 Nanoparticles with Tunable Size

Tian-Sheng CHENG1,2,3, Jiong PAN4, Ying-Ying XU1,2,3, Qun-Qun BAO1,2,3, Ping HU1、*, and Jian-Lin SHI1、*
Author Affiliations
  • 1State Key Laboratory of High Performance Ceramics and Superfine Microstructures, Shanghai Institute of Ceramics, Chinese Academy of Sciences, Shanghai 200050, China
  • 2University of Chinese Academy of Sciences, Beijing 100049, China
  • 3Shanghai Tech University, Shanghai 201210, China
  • 4Tongji University, Shanghai 200092, China
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    TEM images of ZnMn-Fe3O4 nanoparticles and histograms of their size distributions obtained by Fe(acac)3, Mn(acac)2 and Zn(acac)2 with (a, c) and without (b, d) adding 1,2-hexadecanediol
    . TEM images of ZnMn-Fe3O4 nanoparticles and histograms of their size distributions obtained by Fe(acac)3, Mn(acac)2 and Zn(acac)2 with (a, c) and without (b, d) adding 1,2-hexadecanediol

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    TEM image (a), histograms of their size distributions (b), high-resolution TEM image (c) and selected area electron diffraction (SAED) pattern (d) of 15 nm-sized ZnMn-Fe3O4 nanoparticles prepared from Fe(acac)3, MnCl2 and ZnCl2
    . TEM image (a), histograms of their size distributions (b), high-resolution TEM image (c) and selected area electron diffraction (SAED) pattern (d) of 15 nm-sized ZnMn-Fe3O4 nanoparticles prepared from Fe(acac)3, MnCl2 and ZnCl2

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    TEM images of 20 nm-sized ZnMn-Fe3O4 nanoparticles synthesized from Fe(acac)3, MnCl2 and ZnCl2 with different reflux time durations of 1.5 h (a) and 2 h (b), and the corresponding histograms of size distributions of 1.5 h (c) and 2 h (d)
    . TEM images of 20 nm-sized ZnMn-Fe3O4 nanoparticles synthesized from Fe(acac)3, MnCl2 and ZnCl2 with different reflux time durations of 1.5 h (a) and 2 h (b), and the corresponding histograms of size distributions of 1.5 h (c) and 2 h (d)

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    XRD patterns (a), FT-IR spectra (b) and energy dispersive X-ray spectroscopy (EDS) data (c) of 5 nm, 10 nm, 15 nm, and 20 nm-sized ZnMn-Fe3O4 nanoparticles
    . XRD patterns (a), FT-IR spectra (b) and energy dispersive X-ray spectroscopy (EDS) data (c) of 5 nm, 10 nm, 15 nm, and 20 nm-sized ZnMn-Fe3O4 nanoparticles

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    Magnetic hysteresis curve (a) and d-1-dependent Ms curve (b) of 5-20 nm-sized ZnMn-Fe3O4 nanoparticles
    . Magnetic hysteresis curve (a) and d-1-dependent Ms curve (b) of 5-20 nm-sized ZnMn-Fe3O4 nanoparticles

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    Tian-Sheng CHENG, Jiong PAN, Ying-Ying XU, Qun-Qun BAO, Ping HU, Jian-Lin SHI. Synthesis of Zn, Mn doped Fe3O4 Nanoparticles with Tunable Size[J]. Journal of Inorganic Materials, 2019, 34(8): 899

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    Paper Information

    Category: RESEARCH LETTERS

    Received: Jan. 6, 2019

    Accepted: --

    Published Online: Sep. 26, 2021

    The Author Email: HU Ping (huping@mail.sic.ac.cn), SHI Jian-Lin (jlshi@mail.sic.ac.cn)

    DOI:10.15541/jim20190013

    Topics

    laser devices and laser physics
    Lasers and Laser Optics
    Laser physics
    laser manufacturing
    Instrumentation, Measurement and Metrology