Journal of the Chinese Ceramic Society, Volume. 52, Issue 5, 1710(2024)
Calcium Silicate Hydrate Gels - A Short Review
[1] [1] DUQUE-REDONDO E, BONNAUD P A, MANZANO H. A comprehensive review of C-S-H empirical and computational models, their applications, and practical aspects[J]. Cem Concr Res, 2022, 156: 106784.
[2] [2] KANTRO D L, BRUNAUER S, WEISE C H. Development of surface in the hydration of calcium silicates. II. extension of investigations to earlier and later stages of hydration[J]. J Phys Chem, 1962, 66(10): 1804-1809.
[3] [3] STADE H, WIEKER W. Cheminform abstract: structure of ill-crystallized calcium hydrogen silicates. I. formation and properties of an ill-crystallized calcium hydrogen disilicate phase[J]. Chemischer Informationsdienst, 1980, 11(42): 8.
[4] [4] RICHARDSON I G, GROVES G W. Models for the composition and structure of calcium silicate hydrate (C-S-H) gel in hardened tricalcium silicate pastes[J]. Cem Concr Res, 1992, 22(6): 1001-1010.
[5] [5] RICHARDSON I G, GROVES G W. The incorporation of minor and trace elements into calcium silicate hydrate (C-S-H) gel in hardened cement pastes[J]. Cem Concr Res, 1993, 23(1): 131-138.
[6] [6] CONG X D, KIRKPATRICK R J. 29Si MAS NMR study of the structure of calcium silicate hydrate[J]. Adv Cem Based Mater, 1996, 3(3/4): 144-156.
[7] [7] MEGAW H D, KELSEY C H. Crystal structure of tobermorite[J]. Nature, 1956, 177(4504): 390-391.
[8] [8] TAYLOR H F W. Proposed structure for calcium silicate hydrate gel[J]. J Am Ceram Soc, 1986, 69(6): 464-467.
[9] [9] BROUWERS H J H. The work of Powers and Brownyard revisited: Part 2[J]. Cem Concr Res, 2005, 35(10): 1922-1936.
[10] [10] FELDMAN R F, SEREDA P J. A model for hydrated Portland cement paste as deduced from sorption-length change and mechanical properties[J]. Matériaux Constr, 1968, 1(6): 509-520.
[11] [11] DAIMON M, ABO-EL-ENEIN S A, ROSARA G, et al. Pore structure of calcium silicate hydrate in hydrated tricalcium silicate[J]. J Am Ceram Soc, 1977, 60(3/4): 110-114.
[12] [12] FELDMAN R, SEREDA P. A model for hydrated Portland cement paste as deduced from sorption-length change and mechanical properties[J]. Matériaux Constru, 1968, 1: 509-520.
[13] [13] JENNINGS H M. A model for the microstructure of calcium silicate hydrate in cement paste[J]. Cem Concr Res, 2000, 30(1): 101-116.
[14] [14] ALLEN A J, THOMAS J J, JENNINGS H M. Composition and density of nanoscale calcium-silicate-hydrate in cement[J]. Nat Mater, 2007, 6(4): 311-316.
[15] [15] JENNINGS H M. Refinements to colloid model of C-S-H in cement: CM-II[J]. Cem Concr Res, 2008, 38(3): 275-289.
[16] [16] GARRAULT S, NONAT A. Hydrated layer formation on tricalcium and dicalcium silicate surfaces: Experimental study and numerical simulations[J]. Langmuir, 2001, 17(26): 8131-8138.
[17] [17] MASOERO E, DEL GADO E, PELLENQ R J M, et al. Nanostructure and nanomechanics of cement: Polydisperse colloidal packing[J]. Phys Rev Lett, 2012, 109(15): 155503.
[18] [18] ALLEN A J, THOMAS J J. Analysis of C-S-H gel and cement paste by small-angle neutron scattering[J]. Cem Concr Res, 2007, 37(3): 319-324.
[19] [19] DOLADO J S, GRIEBEL M, HAMAEKERS J, et al. The nano-branched structure of cementitious calcium-silicate-hydrate gel[J]. J Mater Chem, 2011, 21(12): 4445-4449.
[20] [20] ROSSEN J E, LOTHENBACH B, SCRIVENER K L. Composition of C-S-H in pastes with increasing levels of silica fume addition[J]. Cem Concr Res, 2015, 75: 14-22.
[21] [21] IOANNIDOU K, PELLENQ R J M, DEL GADO E. Controlling local packing and growth in calcium-silicate-hydrate gels[J]. Soft Matter, 2014, 10(8): 1121-1133.
[22] [22] SCRIVENER K L, NONAT A. Hydration of cementitious materials, present and future[J]. Cem Concr Res, 2011, 41(7): 651-665.
[23] [23] MCDONALD P J, RODIN V, VALORI A. Characterisation of intra- and inter-C-S-H gel pore water in white cement based on an analysis of NMR signal amplitudes as a function of water content[J]. Cem Concr Res, 2010, 40(12): 1656-1663.
[24] [24] BRISARD S, CHAE R S, BIHANNIC I, et al. Morphological quantification of hierarchical geomaterials by X-ray nano-CT bridges the gap from nano to micro length scales[J]. Am Mineral, 2012, 97(2/3): 480-483.
[25] [25] GARTNER E M. A proposed mechanism for the growth of C-S-H during the hydration of tricalcium silicate[J]. Cem Concr Res, 1997, 27(5): 665-672.
[26] [26] XU Z, VIEHLAND D. Observation of a mesostructure in calcium silicate hydrate gels of Portland cement[J]. Phys Rev Lett, 1996, 77(5): 952-955.
[27] [27] VIEHLAND D, LI J F, YUAN L J, et al. Mesostructure of calcium silicate hydrate (C-S-H) gels in Portland cement paste: short-range ordering, nanocrystallinity, and local compositional order[J]. J Am Ceram Soc, 1996, 79(7): 1731-1744.
[28] [28] ZHANG X Z, CHANG W Y, ZHANG T J, et al. Nanostructure of calcium silicate hydrate gels in cement paste[J]. J Am Ceram Soc, 2000, 83(10): 2600-2604.
[30] [30] XU Wen, WU Xiaolei. Bull Chin Ceram Soc , 2018, 37(4): 1294-1298.
[32] [32] PENG Xiaoqin, HE Lijuan, LIU Yanmeng. J Chongqing Univ Nat Sci Ed, 2005, 28(5): 59-62.
[34] [34] HE Ciquan, DU Haiyan, SUN Jiayue. New Chem Mater, 2007, 35(10): 19-21.
[36] [36] LIU Zhen, LIANG Wei, XU Bingshe, et al. Mater Sci Technol, 2000, 8(3): 103-108.
[37] [37] RICHARDSON I G, BROUGH A R, BRYDSON R, et al. Location of aluminum in substituted calcium silicate hydrate (C-S-H) gels as determined by 29Si and 27Al NMR and EELS[J]. J Am Ceram Soc, 1993, 76(9): 2285-2288.
[38] [38] GRUTZECK M W, ROY D M. Electron microprobe studies of the hydration of 3CaO.SiO2[J]. Nature, 1969, 223(5205): 492-494.
[40] [40] SHI Lei, MA Suhua, LI Weifeng, et al. Concrete, 2013(11): 101-104.
[42] [42] HE Y J, ZHAO X G, LU L N, et al. Effect of C/S ratio on morphology and structure of hydrothermally synthesized calcium silicate hydrate[J]. J Wuhan Univ Technol Mater Sci Ed, 2011, 26(4): 770-773.
[43] [43] OKADA Y, ISHIDA H, MITSUDA T. 29Si NMR spectroscopy of silicate anions in hydrothermally formed C-S-H[J]. J Am Ceram Soc, 1994, 77(3): 765-768.
[44] [44] KLUR I, POLLET B, VIRLET J, et al. C-S-H structure evolution with calcium content by multinuclear NMR[C]//COLOMBET P, ZANNI H, GRIMMER AR, et al. Nuclear Magnetic Resonance Spectroscopy of Cement-Based Materials. Berlin, Heidelberg: Springer, 1998: 119-141.
[46] [46] FAN Fuzhong, QIAN Guangren, LAI Zhenyu, et al. Bull Chin Ceram Soc, 2001, 20(1): 18-23.
[48] [48] XU Guangliang, LAI Zhenyu, QIAN Guangren, et al. J Chin Ceram Soc, 2000, 28(2): 100-104.
[49] [49] QIAN G R, XU G L, LI H Y, et al. Mg-xonotlite and its coexisting phases[J]. Cem Concr Res, 1997, 27(3): 315-320.
[51] [51] ZDZISLAW PYTEL, ZHAO Shixi. Sci Technol Overseas Build Mater, 1999, 20(3): 47-49.
[52] [52] BALTAKYS K, EISINAS A, DONELIENE J, et al. The hydrothermal synthesis of calcium aluminium silicate hydrates and its application on portiland cement hydration[J]. Rev Rom Mater, 2015, 45(3): 218.
[53] [53] NOCUò-WCZELIK W. Effect of Na and Al on the phase composition and morphology of autoclaved calcium silicate hydrates [J]. Cem Concr Res, 1999, 29(11): 1759-1767.
[55] [55] KE Changjun. Sci Technol Overseas Build Mater, 2007, 28(4): 37-40.
[56] [56] WIEKER W, GRIMMER A R, WINKLER A, et al. Solid-state high-resolution 29Si NMR spectroscopy of synthetic 14 ?, 11 ? and 9 ? tobermorites[J]. Cem Concr Res, 1982, 12(3): 333-339.
[57] [57] FAUCON P, CHARPENTIER T, NONAT A, et al. Triple-quantum two-dimensional 27Al magic angle nuclear magnetic resonance study of the aluminum incorporation in calcium silicate hydrates[J]. J Am Chem Soc, 1998, 120(46): 12075-12082.
[58] [58] STADE H. On the reaction of C-S-H(di, poly) with alkali hydroxides[J]. Cem Concr Res, 1989, 19(5): 802-810.
[60] [60] TONG Xueli, LIU Gongcheng. J Chin Ceram Soc, 1963(3): 129-138.
[62] [62] JI Fangying, GUAN Wei, ZHOU Weiwei, et al. Chin J Environ Eng, 2014, 8(2): 493-498.
[64] [64] LEI Yongsheng, HAN Tao, WANG Huiqi, et al. Bull Chin Ceram Soc, 2014, 33(3): 465-469.
[66] [66] ZENG Lu, HE Mu, MAO Ding. Non Met Mines, 2017, 40(3): 10-13.
[67] [67] GALLUCCI E, ZHANG X, SCRIVENER K L. Effect of temperature on the microstructure of calcium silicate hydrate (C-S-H)[J]. Cem Concr Res, 2013, 53: 185-195.
[68] [68] WANG S P, PENG X Q, TANG L P, et al. Influence of hydrothermal synthesis conditions on the formation of calcium silicate hydrates: from amorphous to crystalline phases[J]. J Wuhan Univ Technol Mater Sci Ed, 2018, 33(5): 1150-1158.
[70] [70] WANG Zheng, YANG Yingzi, LI Jiahe. Mater Sci Technol, 2007, 15(6): 789-791.
[72] [72] LI Yuanzhong, TANG Erzhuo. J Chin Ceram Soc, 1991, 19(4): 373-380.
[73] [73] MATSCHEI T, LOTHENBACH B, GLASSER F P. The role of calcium carbonate in cement hydration[J]. Cem Concr Res, 2007, 37(4): 551-558.
[74] [74] YAMADA K, TAKAHASHI T, HANEHARA S, et al. Effects of the chemical structure on the properties of polycarboxylate-type superplasticizer[J]. Cem Concr Res, 2000, 30(2): 197-207.
[75] [75] RAN Q P, SOMASUNDARAN P, MIAO C W, et al. Effect of the length of the side chains of comb-like copolymer dispersants on dispersion and rheological properties of concentrated cement suspensions[J]. J Colloid Interface Sci, 2009, 336(2): 624-633.
[76] [76] ALIZADEH R, RAKI L, MAKAR J M, et al. Hydration of tricalcium silicate in the presence of synthetic calciuma silicatea hydrate[J]. J Mater Chem, 2009, 19(42): 7937-7946.
[78] [78] PENG Xiaoqin, LAN Cong, WANG Shuping, et al. J Build Mater, 2015, 18(2): 195-201.
[80] [80] YU Lincen, WANG Weishan, ZHENG Baicun. New Build Mater, 2018, 45(10): 35-38.
[81] [81] ARTIOLI G, VALENTINI L, DALCONI M C, et al. Imaging of nano-seeded nucleation in cement pastes by X-ray diffraction tomography[J]. Int J Mater Res, 2014, 105(7): 628-631.
[83] [83] ZHANG Chaoyang, CAI Yi, KONG Xiangming, et al. J Chin Ceram Soc, 2019, 47(5): 585-593.
[85] [85] ZHANG Hongsen, GUO Yutong, JIANG Baojiang, et al. J Heilongjiang Univ Sci Technol, 2018, 28(1): 65-69.
[87] [87] ZHAO Yue, ZHENG Xin, XU Chang, et al. J Saf Environ, 2017, 17(5): 1904-1908.
[88] [88] OKANO K, UEMOTO M, KAGAMI J, et al. Novel technique for phosphorus recovery from aqueous solutions using amorphous calcium silicate hydrates (A-CSHs)[J]. Water Res, 2013, 47(7): 2251-2259.
[89] [89] MAEDA H, ISHIDA E H. Hydrothermal preparation of diatomaceous earth combined with calcium silicate hydrate gels[J]. J Hazard Mater, 2011, 185(2/3): 858-861.
[90] [90] KHRAISHEH M A M, AL-GHOUTI M A, ALLEN S J, et al. Effect of OH and silanol groups in the removal of dyes from aqueous solution using diatomite[J]. Water Res, 2005, 39(5): 922-932.
[92] [92] SHI Yongliang, HAN Rui. New Build Mater, 2020, 47(11): 60-63.
[94] [94] CHENG Zhaoxia, PENG Xiaoqin, JI Xiaoli, et al. Non Met Mines, 2016, 39(6): 7-10.
[96] [96] GOU Jing, PENG Xiaoqin, RAN Peng, et al. Bull Chin Ceram Soc, 2019, 38(10): 3309-3313.
[98] [98] PENG Xiaoqin, GU Shuying, HUANG Tao, et al. J Civ Archit Environ Eng, 2010, 32(5): 109-113.
[100] [100] LIU Qinfu, ZHANG Shilong, JI Leibo, et al. New Chem Mater, 2013, 41(6): 162-166.
[102] [102] WU Pan, ZHANG Meiyun, WANG Jian, et al. China Pulp Pap, 2012, 31(12): 27-31.
[103] [103] AUGUSTYNIAK A, SIKORA P, JABLONSKA J, et al. The effects of calcium-silicate-hydrate (C-S-H) seeds on reference microorganisms[J]. Appl Nanosci, 2020, 10(12): 4855-4867.
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ZHAO Piqi, SUN Qian, YANG Xinyue, LU Lingchao, CHENG Xin. Calcium Silicate Hydrate Gels - A Short Review[J]. Journal of the Chinese Ceramic Society, 2024, 52(5): 1710
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Received: Jul. 26, 2023
Accepted: --
Published Online: Aug. 20, 2024
The Author Email: Piqi ZHAO (mse-zhaopq@ujn.edu.cn)