Journal of Inorganic Materials, Volume. 39, Issue 10, 1135(2024)

Activated Sludge Incineration Ash Derived Fenton-like Catalyst: Preparation and Degradation Performance on Methylene Blue

Mengyu CAI... Hongmiao LI-YANG, Caiyun YANG, Yuting ZHOU and Hao WU* |Show fewer author(s)
Author Affiliations
  • Hebei Key Laboratory of Heavy Metal Deep-Remediation in Water and Resource Reuse, School of Environmental and Chemical Engineering, Yanshan University, Qinhuangdao 066004, China
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    Figures & Tables(12)
    XRD patterns of SD, FSD and RFSD
    SEM images of (a, b) SD and (c, d) FSD before and after loading Fe2+
    MB degradation performances in different systems
    Effects of (a) concentration of Fe2+ loading solution, (b) oxidant dosage and (c) catalyst dosage on degradation of MB by FSD/PAA system
    Effect of different quenchers on degradation of MB by the optimized FSD/PAA system
    (a, b) Total and (c, d) Fe2p XPS spectra of (a, c) FSD and (b, d) RFSD before and after catalytical reaction
    Degradation pathways and intermediates of MB in the FSD/PAA system
    Effects of co-existed substrates and water conditions on the degradation of MB by the optimized FSD/PAA system
    Degradation performance of different pollutants by FSD/PAA system during 20 min
    Effect of pH on the degradation of MB by the FSD/PAA system
    • Table 1. Characterizations of different water samples

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      Table 1. Characterizations of different water samples

      ItemTWLWWastewater
      TOC/(mg·L-1)16.728.8188.1
      F-/(mg·L-1)0.10.10.2
      Cl-/(mg·L-1)23.224.351.1
      K+/(mg·L-1)30.935.664.4
      Mg2+/(mg·L-1)16.721.496.5
    • Table 2. HPLC conditions for phase gradient elution measuring concentrations of organic contaminants

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      Table 2. HPLC conditions for phase gradient elution measuring concentrations of organic contaminants

      CompoundColumn temperature/℃ Flow rate/(mL·min-1) Wavelength/nm Phase mobile phasePhase elution gradient
      MB400.2254Ammonium acetate (A)+ acetonitrile (B)0-1-9-14 min, 10%B-10%B-90%B-90%B
      SMX400.32750.1% Formic acid solution (A)+ methanol (B)0-1-1-3.5-5 min, 20%B-20%B-51.25%B-51.25%B
      GM400.32780.1% Formic acid solution (A)+ acetonitrile (B)0-0.5-1-4-6 min, 5%B-5%B-30%B-30%B
      MDZ400.8318Ultrapure water (A)+ acetonitrile (B)0-0.5-3-5 min, 6%B-5%B-20%B-90%B
      CIP400.3278Ultrapure water (A)+ acetonitrile (B)0-0.5-3-5 min, 6%B-5%B-20%B-90%B
      RHB400.25540.1% Formic acid solution (A)+ acetonitrile (B)0-5-8 min, 5%B-95%B-95%B
      TC400.3360Ultrapure water (A)+ acetonitrile (B)0-0.5-3-5 min, 6%B-5%B-20%B-90%B
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    Mengyu CAI, Hongmiao LI-YANG, Caiyun YANG, Yuting ZHOU, Hao WU. Activated Sludge Incineration Ash Derived Fenton-like Catalyst: Preparation and Degradation Performance on Methylene Blue[J]. Journal of Inorganic Materials, 2024, 39(10): 1135

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    Paper Information

    Category:

    Received: Dec. 18, 2023

    Accepted: --

    Published Online: Dec. 13, 2024

    The Author Email: WU Hao (hwu@ysu.edu.cn)

    DOI:10.15541/jim20230580

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