Spectroscopy and Spectral Analysis, Volume. 42, Issue 6, 1928(2022)

Study on Metallic Samples Determination Based on Prompt Gamma Neutron Activation Analysis Technique

Can CHENG1,1;... Da-qian HEI2,2; *;, Wen-bao JIA1,1;, Qing SHAN1,1;, Yong-sheng LING1,1; and Dong ZHAO1,1; |Show fewer author(s)
Author Affiliations
  • 11. Department of Nuclear Science and Technology, College of Materials Science and Technology, Nanjing University of Aeronautics and Astronautics, Nanjing 211106, China
  • 22. School of Nuclear Science and Technology, Lanzhou University, Lanzhou 730000, China
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    Figures & Tables(9)
    Schematic diagram of the designed PGNAA system(a): Top view; (b): Side view
    The background spectrum of system(a): 450~1 000 keV; (b): 1 000~2 000 keV; (c): 2 000~4 500 keV
    Prompt gamma-ray spectra and peaks fitting of the meatal samples(a): Spectra of Fe; (b): Peaks fitting of Fe; (c): Spectra of Ti; (d): Peaks fitting of Ti; (e): Spectra of Cr; (f): Peaks fitting of Cr; (g): Spectra of Ni; (h): Peaks fitting of Ni; (i): Spectra of Cu; (j): Peaks fitting of Cu
    The calibration curve of metal samples(a): Fe; (b): Ti; (c): Cr; (d): Ni; (e): Cu
    • Table 1. Parameters and energies of prompt gamma-rays of Fe, Ti, Cr, Ni and Cu

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      Table 1. Parameters and energies of prompt gamma-rays of Fe, Ti, Cr, Ni and Cu

      元素编号:尺寸(L1×L2×L3)/cm3质量/g/keV
      Fe#1: 1×4×4
      #2: 2×4×4
      #3: 3×4×4
      #4: 4×4×4
      123.36, 246.50, 369.99, 493.11846.8
      Ti71.07, 142.21, 213.31, 284.44983.5
      Cr113.99, 228.14, 342.76, 456.881 434.2
      Ni143.28, 286.07, 429.44, 572.901 454.3
      Cu141.41, 282.71, 423.94, 565.25962
    • Table 2. Parameters of stainless steel standard samples

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      Table 2. Parameters of stainless steel standard samples

      标准样品直径×高度/cm×cmFe/Wt%Cr/Wt%
      YSBS3738853.8124.33
      YSBS373783.5×3.571.2018.08
      YSBS3738682.5611.76
    • Table 3. Detection efficiencies of HPGe detector for different samples

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      Table 3. Detection efficiencies of HPGe detector for different samples

      样品
      编号
      探测效率
      FeTiCrNiCu
      #18.97×10-39.16×10-36.64×10-36.28×10-38.11×10-3
      #27.40×10-38.33×10-35.79×10-35.28×10-36.63×10-3
      #36.39×10-37.75×10-35.19×10-34.63×10-35.69×10-3
      #45.76×10-37.35×10-34.80×10-34.20×10-35.11×10-3
    • Table 4. The MDL of different metal samples

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      Table 4. The MDL of different metal samples

      元素MDL/g
      Fe44
      Ti25
      Cr33
      Ni108
      Cu72
    • Table 5. Determination results of unknown stainless steel sample

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      Table 5. Determination results of unknown stainless steel sample

      元素PGNAA校准曲线PGNAA检测结果/(Wt%)XRF校准曲线XRF检测结果/(Wt%)偏差/%
      Fey=14.13x71.54±3.73y=423.80x-4 32574.46±4.674.08
      Cry=26.72x15.14±1.08y=485.97x+2 45214.69±1.32-2.97
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    Can CHENG, Da-qian HEI, Wen-bao JIA, Qing SHAN, Yong-sheng LING, Dong ZHAO. Study on Metallic Samples Determination Based on Prompt Gamma Neutron Activation Analysis Technique[J]. Spectroscopy and Spectral Analysis, 2022, 42(6): 1928

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    Paper Information

    Category: Research Articles

    Received: May. 25, 2021

    Accepted: --

    Published Online: Nov. 14, 2022

    The Author Email:

    DOI:10.3964/j.issn.1000-0593(2022)06-1928-06

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