<trans-title>Powder Characteristics on the Rheological Performance of Resin-based Zirconia Suspension for Stereolithography</trans-title>

Xing-Bang LI; He ZHONG; Jing-Xian ZHANG; Yu-Sen DUAN; Dong-Liang JIANG

doi:10.15541/jim20190091

Journal of Inorganic Materials, Volume. 35, Issue 2, 231(2020)

Powder Characteristics on the Rheological Performance of Resin-based Zirconia Suspension for Stereolithography

Xing-Bang LI1...2, He ZHONG1, Jing-Xian ZHANG1,3,*, Yu-Sen DUAN1,2 and Dong-Liang JIANG1 |Show fewer author(s)

¹State Key Laboratory of High Performance Ceramics and Superfine Microstructure, Shanghai Institute of Ceramics, Chinese Academy of Sciences, Shanghai 200050, China

²University of Chinese Academy of Sciences, Beijing 100049, China

³Suzhou Institute of SICCAS (Shanghai Institute of Ceramics, Chinese Academy of Sciences), Taicang 215499, China

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Figures & Tables(10)

. Viscosity as a function of shear rate for 35vol% dispersions with different powders

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. Rheological curves of slurries using powders with (a) similar particle size distribution and (b) similar specific surface area

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. SEM images of (a) No. 7 powder, (b) No. 5 powder and (c) No. 9 powder

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. Rheological behavior of slurries with different solid loadings

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. Relative viscosity of slurries as a function of solid loading at the shear rate of 30 s^-1

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. Optical pictures of green (a) and sintered (b) zirconia parts fabricated by stereolithography

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$SEM image of the fracture surface of the sintered part$

. SEM image of the fracture surface of the sintered part

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Table 1.
Basic information of the raw powders used in this work

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Table 1.
Basic information of the raw powders used in this work

No.	Product name	Supplier
1	SZ-DT-SE2	Jiangxi Size Materials Co., Ltd.
2	YH-3YSZ	Yixingshi Yihui Naimo Cailiao Co., Ltd.
3	SG-3YB-S₂Z₀-E	Dongguan CSG Ceramics Technology Co., Ltd.
4	OZ-3Y-6	Guangdong Orient Zirconic Ind Sci & Tech Co., Ltd.
5	TYSZ-3-S	Hubei Jing Gui Zirconium Co., Ltd.
6	HWYA-N-3S	GuangDong Huawang Zirconium Materials Co., Ltd.
7	G3Y-020OO	Shandong Sinocera Functional Material Co., Ltd.
8	SZ-DM-3.0-F3	Jiangxi Size Materials Co., Ltd.
9	TZ-3YSE	Tosoh Corp., Tokyo, Japan

Table 2.
Particle size and distribution of No. 9 powder before and after ball milling
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Table 2.
Particle size and distribution of No. 9 powder before and after ball milling
Powder d₁₀/nm d₅₀/nm d₉₀/nm
Before roll milling 196.7 316.9 510.3
After roll milling 207.0 318.0 488.4

Table 3.
Particle size distribution and BET specific surface area of raw powders

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Table 3.
Particle size distribution and BET specific surface area of raw powders

No.	d₁₀/nm	d₅₀/nm	d₉₀/nm	S_BET/(m²·g^-1)	Slurry viscosity/(Pa·s)
1	172.7	283.3	464.6	15.596	67.2
2	323.2	577.6	1032.3	8.643	43.8
3	146.0	252.4	436.5	15.712	22.6
4	180.3	309.1	529.9	17.521	18
5	229.0	390.3	665.3	8.194	14.5
6	140.1	206.6	304.5	9.236	14
7	236.5	386.4	631.4	9.18	11.7
8	169.2	300.0	531.7	10.188	11
9	196.7	316.9	510.3	7.133	9

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Xing-Bang LI, He ZHONG, Jing-Xian ZHANG, Yu-Sen DUAN, Dong-Liang JIANG. Powder Characteristics on the Rheological Performance of Resin-based Zirconia Suspension for Stereolithography[J]. Journal of Inorganic Materials, 2020, 35(2): 231

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Paper Information

Category: RESEARCH LETTERS

Received: Mar. 1, 2019

Accepted: --

Published Online: Jan. 27, 2021

The Author Email: ZHANG Jing-Xian (jxzhang@mail.sic.ac.cn)

DOI:10.15541/jim20190091

Topics

laser devices and laser physics

Lasers and Laser Optics

Laser physics

laser manufacturing

Instrumentation, Measurement and Metrology

Table 1. Basic information of the raw powders used in this work

Table 1. Basic information of the raw powders used in this work

Table 2. Particle size and distribution of No. 9 powder before and after ball milling

Table 2. Particle size and distribution of No. 9 powder before and after ball milling

Table 3. Particle size distribution and BET specific surface area of raw powders

Table 3. Particle size distribution and BET specific surface area of raw powders

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Table 1.
Basic information of the raw powders used in this work

Table 1.
Basic information of the raw powders used in this work

Table 2.
Particle size and distribution of No. 9 powder before and after ball milling

Table 2.
Particle size and distribution of No. 9 powder before and after ball milling

Table 3.
Particle size distribution and BET specific surface area of raw powders

Table 3.
Particle size distribution and BET specific surface area of raw powders