Spectroscopy and Spectral Analysis, Volume. 40, Issue 10, 3153(2020)

Chemical Compositions of Carbon Sources Affected on Surface Morphology and Spectral Properties of the Synthetic Carbon Microspheres

Yu-na KAN*... Bing-wei CHEN, Sheng-cheng ZHAI and Chang-tong MEI |Show fewer author(s)
Author Affiliations
  • College of Materials Science and Engineering, Nanjing Forestry University, Nanjing 210037, China
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    Figures & Tables(8)
    The optical micrograph and ultraviolet excitation autofluorescence images of the cross section of the Vitis vinifera (a, c) and Eupatorium adenophorum (b, d)
    SEM images of carbon microspheres by using xylose (a), glucose (b), and sucrose (c) as carbon sources and their size distribution (d)
    SEM images and size distribution of carbon microspheres by using Vitis vinifer(a, c) and Eupatorium adenophorum (b, d) as carbon sources
    FTIR spectra of biomass raw material and carbon microspheres prepared from biomass material (a) and FTIR spectra of carbon microspheres prepared from different carbon sources (b)Biomass raw materials: v: Vitis vinifera; e: Eupatorium adenophorum; Carbon microspheres: c-v: Vitis vinifera; c-e: Eupatorium adenophorum; c-x: xylose; c-g: glucose; c-s: sucrose
    Score plot (a) and loading plot (b) of principle component analysis of carbon microspheres
    XPS of C(1s) (a) and O(1s) (b) curving fitting for glucose carbon spheres
    • Table 1. The chemical composition and hydrolysis efficiency of the biomass material

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      Table 1. The chemical composition and hydrolysis efficiency of the biomass material

      原料原料化学组分含量/%*固体脱除
      率/%a
      各组分脱除率/%b
      纤维素半纤维素木质素纤维素半纤维素木质素
      葡萄藤原料36.35(0.34)20.64(0.23)28.09(0.38)14.469.3911.6314.00
      残渣38.51(0.05)21.32(0.58)28.25(0.07)
      紫茎泽兰原料38.58(0.02)19.20(0.22)24.58(0.29)35.9421.8234.1633.60
      残渣44.23(0.01)19.74(0.08)25.48(0.42)
    • Table 2. Band assignments for FTIR spectrum of the different carbon microspheres

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      Table 2. Band assignments for FTIR spectrum of the different carbon microspheres

      吸收范围/cm-1峰位归属
      2 927C—HX伸缩振动(烷基、 脂肪族和芳香族)
      1 700C=O伸缩振动(羧基、 羰基)
      1 605芳香环的骨架振动
      1 515芳香环的骨架振动
      1 460~1 000—OH面外弯曲振动(芳香环); C—O—C的振动(羟基、 酯基或醚基)
      1 020C—O—C振动峰(芳醚)
      793, 756芳香环外平面C—H变形
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    Yu-na KAN, Bing-wei CHEN, Sheng-cheng ZHAI, Chang-tong MEI. Chemical Compositions of Carbon Sources Affected on Surface Morphology and Spectral Properties of the Synthetic Carbon Microspheres[J]. Spectroscopy and Spectral Analysis, 2020, 40(10): 3153

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    Paper Information

    Category: Research Articles

    Received: Sep. 2, 2019

    Accepted: --

    Published Online: Jun. 18, 2021

    The Author Email: KAN Yu-na (1461390279@qq.com)

    DOI:10.3964/j.issn.1000-0593(2020)10-3153-08

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