Journal of Inorganic Materials, Volume. 35, Issue 5, 601(2020)

Preparing Biomedical CaCO3/HA Composite with Oyster Shell

Ziyang LIU... Zhen GENG and Zhaoyang LI |Show fewer author(s)
Author Affiliations
  • School of Materials Science and Engineering, Tianjin University, Tianjin 300350, China
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    Figures & Tables(10)
    (a) XRD pattern, (b) EDS analysis, (c) SEM micrograph and (d) TEM image and SAED pattern of the powders prepared by heating and washing the oyster shell
    XRD patterns of of the synthesized samples
    SEM micrographs of the hydrothermally synthesized samples
    TEM and HRTEM images of the hydrothermally synthesized samples
    Specific surface area of the prepared samples
    TG curves of the prepared samples
    SEM micrographs of the samples after degradation
    • Table 1. Heavy metal content of the calcined products of oyster shells

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      Table 1. Heavy metal content of the calcined products of oyster shells

      ElementCalcined product /(mg·kg-1)Limit/(mg·kg-1)
      Pb<1030
      Cd<1.55
      Hg<15
      As<13
    • Table 2. Ca and P concentrations and HA transition degree of samples

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      Table 2. Ca and P concentrations and HA transition degree of samples

      20%HA40%HA60%HA
      Concentration of Ca/(mg·L-1)(19.91±0.72)(20.00±1.08)(20.02±0.52)
      Concentration of P/(mg·L-1)(1.62±0.17)(3.19±0.22)(4.02±0.19)
      Degree of HA transition/%(17.5±0.57)(34.3±1.02)(43.2±0.33)
    • Table 3. Ca2+ concentration and degradation rate of samples

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      Table 3. Ca2+ concentration and degradation rate of samples

      20%HA40%HA60%HACaCO3
      Degradation time/dConcentration of Ca2+/(mg·L-1)Degradation rate/%Concentration of Ca2+/(mg·L-1)Degradation rate/%Concentration of Ca2+/(mg·L-1)Degradation rate/%Concentration of Ca2+/(mg·L-1)Degradation rate/%
      7(16.13±0.40)8.1(13.39±0.23)6.7(11.61±0.92)5.8(18.93±0.17)9.8
      14(30.26±1.12)15.2(24.02±0.83)12.0(21.62±1.36)10.8(42.70±0.19)22.1
      21(43.20±1.47)21.7(33.40±1.38)16.2(28.11±1.07)14.3(56.41±0.32)29.2
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    Ziyang LIU, Zhen GENG, Zhaoyang LI. Preparing Biomedical CaCO3/HA Composite with Oyster Shell[J]. Journal of Inorganic Materials, 2020, 35(5): 601

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    Paper Information

    Category: RESEARCH PAPER

    Received: Apr. 4, 2019

    Accepted: --

    Published Online: Mar. 1, 2021

    The Author Email:

    DOI:10.15541/jim20190144

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