Journal of Inorganic Materials, Volume. 38, Issue 11, 1345(2023)

Consolidation of Fragile Weathered Bone Relics Using Hydroxyapatite Material as Consolidant

Yan LIU1...2,3, Yufan ZHANG1,2,3, Ximan WANG1,2,3, Ting LI1,2,3, Wenting MA1,2,3, Fuwei YANG1,2,3,*, Liang CHEN1,2,3, Dongyue ZHAO1,2,3, and Xiaoqin YAN1,23 |Show fewer author(s)
Author Affiliations
  • 11. China-Central Asia “the Belt and Road” Joint Laboratory on Human and Environment Research, Northwest University, Xi’an 710127, China
  • 22. Key Laboratory of Cultural Heritage Research and Conservation, Northwest University, Xi’an 710127, China
  • 33. School of Culture Heritage, Northwest University, Xi’an 710127, China
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    Figures & Tables(18)
    Calcium oxide-calcium hydrogen phosphate dispersion in alcohol at concentration of 25%
    Consolidation mechanism of weathered bones using calcium oxide-calcium hydrogen phosphate dispersion in alcohol as consolidant
    Color difference of fragile bone samples after consolidation treatment
    Effects of consolidation way and consolidant ratio on the bone weight increment
    Effects of consolidation way and consolidant ratio on the bone porosity
    Effects of consolidation way and consolidant ratio on the bone density
    Effects of consolidation method and consolidant ratio on surface strength of the bones
    Morphology of fragile bone sample before consolidation treatment
    Morphologies of fragile bone samples after consolidation treatments with mass ratios of calcium oxide to calcium hydrogen phosphate at 1 : 1 (a), 1 : 3 (b), 1 : 4 (c), 1 : 5 (d), 1 : 6 (e) and 1 : 7 (f), respectively
    EDS analysis results of fragile bone samples before and after consolidation treatment
    Cross-sectional topographies of fragile bone samples before and after consolidation treatments
    Cross-sectional topographies of fragile bone samples treated by different mass ratios of calcium oxide to calcium hydrogen phosphate
    XRD results of bones before (a) and after (b) consolidation treatment
    Effect of consolidant ratio on final product
    Photos of archaeological bone before (a) and after (b) consolidation treatment
    • Table 1. Experimental groups of different mass ratios

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      Table 1. Experimental groups of different mass ratios

      GroupMass ratio
      1 : 11 : 31 : 41 : 51 : 61 : 7
      Brushing123456
      Soaking789101112
      Dripping131415161718
    • Table 2. EDS analysis results of frgile bone before and after consolidation treatment

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      Table 2. EDS analysis results of frgile bone before and after consolidation treatment

      ElementWeight ratio before consolidation/%Weight ratio after consolidation/%
      C05.62
      O56.9356.32
      Na9.572.56
      Mg0.911.12
      P12.0413.23
      Ca20.5521.15
      Total100.00100.00
    • Table 3. Phases of produts under different consolidant ratios

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      Table 3. Phases of produts under different consolidant ratios

      Ratio of CaO : CaHPO4Ca(OH)2CaHPO4Ca5(PO)4OH
      1 : 1+++-++
      1 : 3--++++
      1 : 4-+++++
      1 : 5-+++++
      1 : 6-++++
      1 : 7-+++++
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    Yan LIU, Yufan ZHANG, Ximan WANG, Ting LI, Wenting MA, Fuwei YANG, Liang CHEN, Dongyue ZHAO, Xiaoqin YAN. Consolidation of Fragile Weathered Bone Relics Using Hydroxyapatite Material as Consolidant[J]. Journal of Inorganic Materials, 2023, 38(11): 1345

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    Paper Information

    Category:

    Received: Nov. 3, 2022

    Accepted: --

    Published Online: Mar. 6, 2024

    The Author Email: YANG Fuwei (yangfuwei@nwu.edu.cn)

    DOI:10.15541/jim20220729

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