Journal of the Chinese Ceramic Society, Volume. 50, Issue 7, 2005(2022)
Effect of Heat-Treatment Temperature on Properties of SiO2f/SiO2 Composites
It is of great practical significance to develop thermal insulation materials with integrated load bearing and thermal insulation for energy saving and emission reduction in high-temperature engineering. In this work, SiO2f/SiO2 composites were prepared by a precursor impregnation heat-treatment method with quartz fiber needled felt as a reinforcement and silica sol as a precursor. The effect of heat-treatment temperature on the density, porosity, mechanical properties and thermal properties of SiO2f/SiO2 composites was investigated. The composition and microstructure of the composites were characterized by X-ray diffraction and scanning electron microscopy. The coefficient of thermal expansion and thermal conductivity of composites were measured by a push rod method and a transient hot-wire method. The results indicate that the apparent porosity and mechanical strength firstly increase and then decrease with the increase of heat-treatment temperature. The sample after heat-treatment at 450 ℃ has the optimum overall performance (i.e., the flexural strength of 23.5 MPa, and the compressive strength of 61.9 MPa). The fracture mechanism is a ductile fracture. At 300-700 ℃, the thermal expansion coefficient of the sample is 0.564×10-6/℃. The thermal conductivity of the samples decreases with the increase of temperature, and it is as low as 0.096 W/m·K at 700℃. The SiO2f/SiO2 composite prepared has some advantages in the integrated application of load bearing and thermal insulation, and meets the harsh requirements of hot pressing and sintering, non-ferrous metallurgy and other industries.
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DING Donghai, LI Runan, ZHANG Li, PENG Kai, XIAO Guoqing, DUAN Feng, DENG Peilin, Li Jie. Effect of Heat-Treatment Temperature on Properties of SiO2f/SiO2 Composites[J]. Journal of the Chinese Ceramic Society, 2022, 50(7): 2005
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Received: Sep. 22, 2021
Accepted: --
Published Online: Dec. 6, 2022
The Author Email: Donghai DING (dingdongxauat@163.com)
CSTR:32186.14.