In order to realize the fast and non-contact detection of oil pollution in costal zone, the ultraviolet laser was used as the exciting source, a system used for oil pollution based on laser-induced-fluorescence (LIF) technology was established. The fluorescence spectra of several oil samples were measured through this system. The measurement results show that there are obvious differences among the fluorescence spectra of these samples, which can be used as a reference for oil pollution classification and recognition.