Bulletin of the Chinese Ceramic Society, Volume. 43, Issue 12, 4563(2024)

Synthesis of Spheroid Ba(Mg1/3Ta2/3)O3 Nano-Powders by Hydrothermal Method

ZUO Chuandong1... WAN Jingqi1, WEI Boxu1, YANG Zaiwen1, ZUO Chuange1 and MA Chaoyang2,* |Show fewer author(s)
Author Affiliations
  • 1Zhongke Haoye Dongguan Material Technology Co., Ltd., Dongguan 523808, China
  • 2Songshan Lake Materials Laboratory, Dongguan 523808, China
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    Barium magnesium tantalate (Ba(Mg1/3Ta2/3)O3, BMT) ceramics has excellent microwave dielectric properties. It's the key point to synthesize BMT nano-powders with well-crystallized, uniform grain, good dispersion for perfect microwave dielectric ceramics. BMT nano-powders were prepared by hydrothermal method using tantalum oxide, magnesium nitrate, and barium nitrate as raw materials, KOH solution and isopropyl alcohol as solvents. The crystal structure, morphology, and particle size of the product were characterized by X-ray diffractometer and scanning electron microscope. The effects of KOH concentration, reaction temperature, and reaction time on BMT powders were investigated. The effect of calcination temperature on BMT powders was studied by differential thermal analysis. The results show that the optimum conditions for the synthesis of BMT nano-powders are KOH concentration 2 mol/L, reaction temperature 200 ℃, reaction time 24 h and calcination temperature 1 000 ℃ after freezing-drying. Under this condition, the obtained BMT nano-powders particles are spherically dispersed, and the particle diameter is about 100 nm. This method can be used as a reference for hydrothermal synthesis of BMT nano-powders.

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    ZUO Chuandong, WAN Jingqi, WEI Boxu, YANG Zaiwen, ZUO Chuange, MA Chaoyang. Synthesis of Spheroid Ba(Mg1/3Ta2/3)O3 Nano-Powders by Hydrothermal Method[J]. Bulletin of the Chinese Ceramic Society, 2024, 43(12): 4563

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    Paper Information

    Category:

    Received: May. 30, 2024

    Accepted: Jan. 10, 2025

    Published Online: Jan. 10, 2025

    The Author Email: Chaoyang MA (machaoyang@sslab.org.cn)

    DOI:

    CSTR:32186.14.

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