Spectroscopy and Spectral Analysis, Volume. 32, Issue 3, 817(2012)
FI-KR Non-Separated Method Coupled with FAAS for the Determination of Fe(Ⅱ) and Fe(Ⅲ) in Water
An FI-KR non-separated method coupled with FAAS for the determination of Fe(Ⅱ) and Fe(Ⅲ) was developed. With 60 s of sampling at a flow rate of 6.0 mL·min-1, EF of 41 for Fe(Ⅲ) and 9 for Fe(Ⅱ) were obtained. The precision(RSD, n=11) for Fe(Ⅲ) and Fe(Ⅱ) was 2.3% and 3.1% at the 0.04 mg·L-1 level respectively. When 0.1 ‰φ TEA was used as masking reagent, the recovery rate for Fe(Ⅲ) and Fe(Ⅱ) was from 97% to 101 % and from 96% to 100% respectively.
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WANG Zhong-yuan, ZHANG Hong-kang, FANG Hong-da, SU Yao-dong, Gauri S Mittal. FI-KR Non-Separated Method Coupled with FAAS for the Determination of Fe(Ⅱ) and Fe(Ⅲ) in Water[J]. Spectroscopy and Spectral Analysis, 2012, 32(3): 817
Received: Jun. 23, 2011
Accepted: --
Published Online: Apr. 16, 2012
The Author Email: Zhong-yuan WANG (zhongyuan764@126.com)